The Open Catalysis Journal
2009, 2 : 166-168Published online 2009 December 31. DOI: 10.2174/1876214X00902010166
Publisher ID: TOCATJ-2-166
Telechelic of Poly (Propylene Oxide) Catalyzed by Maghnite-H+
Laboratoire de Chimie des
Polymères, Département de Chimie, Faculté des Sciences, Université
d'Oran Es-Sènia BP N° 1524 El M'Naouar, 31000 Oran, Algeria.
ABSTRACT
Telechelic poly (propylene oxide) (PPO) bismacromonomers bearing methyl Acetate end groups, were prepared by cationic ring-opening polymerization of propylene oxide (PO), in the presence of Acetic anhydride, catalyzed by Maghnite-H+(Mag-H+), in bulk. Mag-H+ is a montmorillonite sheet silicate clay which was exchanged with protons.
The influence of the amount of acetic anhydride and the reaction time on The polymerisation yield and molecular weight were studied. The products have been caracterized by Nuclear magnetic resonance (1H-NMR).